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Correlation and influence of antioxidant compounds of peels and pulps of different species of cacti from Brazilian Caatinga biome using principal component analysis 1 1. Introduction 1 2. Materials and methods 2 2.1. Reagents and standards 2 2.2. Preparation of the extracts 2 2.3. Total phenolic content (TPC) 2 2.4. Antioxidant activity 2 2.4.1. DPPH. assay 2 2.4.2. Ferric reducing antioxidant power (FRAP) 2 2.4.3. β-carotene-linoleic acid assay 2 2.5. High performance liquid chromatography (HPLC) analyses 3 2.6. Statistical analysis 3 3. Results and discussion 3 3.1. Determination of the total phenolic compounds (TPC) 3 3.2. Antioxidant assays 4 3.2.1. DPPH. free radical scavenging activity 4 3.2.2. Ferric reducing antioxidant power (FRAP) 4 3.2.3. β-carotene-linoleic acid assay 5 3.3. Phenolic composition by HPLC 5 3.4. Principal component analysis (PCA) 6 4. Conclusion 8 Data availability 8 Compliance with ethics requirements 8 Human and animal rights 8 Declaration of Competing Interest 8 Acknowledgements 8 Supplementary materials 8 References 8
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