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Ultrasound-assisted production of biodiesel from field pennycress (Thlaspi arvense L.) seeds: Process optimization and qual ... 1 1 Introduction 1 2 Experimental 3 2.1 Materials and reagents 3 2.2 Soxhlet extraction of pennycress seed oil 3 2.3 Ultrasound-assisted extraction of pennycress seed oil 3 2.4 Ultrasound-assisted transesterification 3 2.5 Magnetic stirring–based transesterification 3 2.6 Process optimization 3 2.7 Physicochemical property characterization 4 2.8 Other characterization techniques 4 2.9 Energy consumption analysis 4 2.10 Data analysis 4 3 Results and discussion 4 3.1 Physicochemical properties of pennycress seed oil 4 3.2 Optimisation of UAE for pennycress seed oil 4 3.2.1 Establishment of mathematical model 4 3.2.2 Evaluation of model adequacy 5 3.2.3 Analysis of response surface plots 5 3.2.4 Verification tests 5 3.3 Optimisation of UAT for biodiesel production 5 3.3.1 Establishment of mathematical model 5 3.3.2 Evaluation of model adequacy 7 3.3.3 Analysis of response surface plots 8 3.3.4 Verification tests 8 3.4 Characterisation 9 3.4.1 Fatty acid profiles of oils 9 3.4.2 Thermal stability of oils 9 3.4.3 Fatty acid composition of biodiesel 9 3.4.4 Ther
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