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Insights into the ethanol solvate form of clarithromycin 1 1 Introduction 1 2 Material and methods 2 2.1 Chemicals 2 2.2 Obtaining CAM form 0 2 2.3 Powder X-ray diffraction (PXRD) 2 2.4 Solid-state NMR spectroscopy (ssNMR) 2 2.5 Fourier- transform infrared (FT-IR) spectroscopy 2 2.6 Confocal microscopy 2 2.7 Differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA) 3 2.8 Solubility studies 3 2.9 Microbiological studies 3 2.10 Physical stability studies 3 3 Results and discussion 3 3.1 Identification and characterization of CAM form 0 in solid state 3 3.1.1 Powder X-ray diffraction (PXRD) 3 3.1.2 Solid-state NMR spectroscopy (ssNMR): 13C CP-MAS spectra and HETCOR experiments 3 3.1.3 Fourier-transform infrared spectroscopy (FT-IR) 5 3.1.4 Confocal microscopy 5 3.2 Solution studies of CAM form 0 5 3.2.1 Solubility study 5 3.2.2 Microbiological evaluation 6 3.3 Physical stability studies 6 4 Conclusions 8 Supporting information 8 Declaration of Competing Interest 8 CRediT authorship contribution statement 8 Acknowledgments 8 Supplementary materials 8 References 9

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Language

UND

Category

nonfiction