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## Materials and Physical Measurements All reagents and solvents were purchased from companies commercially and used without further purification. Thermogravimetric analysis (TGA) was measured from 30 °C to 800 °C under a nitrogen (N 2 ) atmosphere with a heating rate of 10°C/min by NETZSCH TG-209. Powder x-ray diffraction (PXRD) data were carried out by Rigaku Ultima IV diffractometer (40 kV, 40 mA, CuKα1, 2 λ = 1.5418 Å), and scanning over the range from 2° to 40° with a step size of 0.02( o ) and a rate of 2°/min. The scanning electron microscopy (SEM) images were obtained on HITACHI S4800. Fourier transform infrared spectra (FT-IR) were recorded on Bruker ALPHAΙ.

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Publisher

American Chemical Society (ACS)

Language

EN

Category

nonfiction