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Preparation of redispersible dry nanoemulsion using chitosan-octenyl succinic anhydride starch polyelectrolyte complex as s ... 1 1 Introduction 1 2 Materials and methods 2 2.1 Materials 2 2.2 Preparation of liquid nanoemulsions 2 2.3 Preparation of feonofibrate spray-dried nanoemulsion powder 3 2.4 Redispersibility study 3 2.5 Characterization of liquid nanoemulsions and redispersed nanoemulsions 3 2.5.1 Droplet size distribution 3 2.5.2 Electrophoretic mobility measurements 3 2.5.3 Transmission electron microscopy (TEM) 3 2.6 Characterizations of fenofibrate spray-dried nanoemulsion powder 3 2.6.1 Determination of spray-dried powder yield 3 2.6.2 Field emission scanning electron microscope (FE-SEM) 3 2.6.3 Fourier transform infrared (FTIR) spectroscopy 3 2.6.4 Raman spectroscopy 3 2.6.5 Differential scanning calorimetry (DSC) 4 2.6.6 Powder X-ray diffraction (PXRD) 4 2.6.7 Drug content determination 4 2.6.8 Dissolution study 4 2.7 Solubility of fenofibrate in dissolution media 4 2.8 High performance liquid chromatography (HPLC) 4 2.9 Statistical analysis 4 3 Results and discussion 4 3.1 Optimization study 4 3.2 Fenofibrate nanoemulsions and spray-dried nanoemulsions 5 3.2.1 Redis

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UND

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nonfiction