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CNTs intercalated graphene oxide with interspersed MoS2 nanoparticles for selective preconcentration and determination of t ... 1 1 Introduction 1 2 Experimental 2 2.1 Chemicals 2 2.2 Synthesis of graphene oxide 2 2.3 Preparation of covalently linked CNT-GO nanocomposite 2 2.4 Fabrication of GO-CNT@MSNP nanosorbent 3 2.5 Sample preparation 3 2.6 Characterization 3 2.7 Optimized batch ‘static” procedure 3 2.8 Optimized column “dynamic” procedure 3 3 Result and discussions 3 3.1 Characterization 3 3.2 Effect of sample pH and adsorption mechanism 5 3.3 Effect of equilibrium time 6 3.4 Effect of sample flow rate in column operation 6 3.5 Eluent and reusability 6 3.6 Effect of co-ions 6 3.7 Preconcentration studies 7 3.8 Analytical method validation 7 3.9 Application: Analysis of real samples 7 4 Conclusion 8 Declaration of Competing Interest 8 Data availability 8 Acknowledgment 8 Appendix A Supplementary data 8 References 8

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EN

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nonfiction