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Ultrasound-assisted dispersive solid-phase extraction for the preconcentration of dyes in water samples 1 1 Introduction 2 2 Experimental 3 2.1 Materials and instrumentation 3 2.2 Synthesis of magnesium ferrite/zinc oxide (MgFe2O4/ZnO) nanocomposite 3 2.2.1 Synthesis of zinc oxide (ZnO) nanoparticles via coprecipitation method 3 2.2.2 Synthesis of magnesium ferrite (MgFe2O4) nanoparticles via self-propagating sol–gel method 3 2.2.3 Synthesis of magnesium ferrite/zinc oxide (MgFe2O4/ZnO) nanocomposite via chemical method 3 2.3 Experimental procedures 3 2.4 Experimental design 4 3 Results and discussion 5 3.1 Characterization of the synthesized nanocomposite 5 3.2 Effects of type of eluent 5 3.3 Effect of the type of mixing 6 3.4 Fitting of the process model and statistical analysis 6 3.5 Study of interactive effects of different parameters on the extraction efficiency 7 3.6 Optimization of extraction conditions 7 3.7 Study of sample volume and preconcentration factor 7 3.8 Analytical performance of the USA-DSPE method 8 3.9 Study of interferences 9 3.10 Reusability of the MgFe2O4/ZnO nanocomposite 9 3.11 Dyes measurement in environmental water samples 9 3.12 Comparison of the presen

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nonfiction