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Upgrading CO2/CH4 separation performances of Pebax-based mixed-matrix membranes incorporated with core/shell-structured ZIF ... 1 1 Introduction 1 2 Experimental 2 2.1 Materials 2 2.2 Preparation of ZIF-L(Co) nanosheets 2 2.3 Preparation of ZIF-L(Co)@ZIF-8 composite nanosheets 2 2.4 Preparation of ZIF-8 nanoparticles 2 2.5 Preparation of ZIF-L(Co)@ZIF-8/Pebax MMMs 2 2.6 Characterization 2 2.7 Gas permeation measurements 2 3 Results and discussion 3 3.1 Formation of ZIF-L(Co)@ZIF-8 composite nanosheets 3 3.2 ZIF-L(Co)@ZIF-8/Pebax MMMs 3 3.3 Gas separation performances 4 3.3.1 Effect of loadings 4 3.3.2 Effect of filler components 5 3.4 Stability of ZIF-L(Co)@ZIF-8/Pebax MMMs 6 3.5 Comparison of separation performances 6 4 Conclusions 6 Author contribution 7 Declaration of competing interest 7 Data availability 7 Acknowledgements 7 Appendix B Supplementary data 7 References 7

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nonfiction