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A defects-free ZIF-90/6FDA-Durene membrane based on the hydrogen bonding/covalent bonding interaction for gas separation 1 1 Introduction 1 2 Experimental 2 2.1 Materials 2 2.2 Preparation of 6FDA-Durene 2 2.3 Preparation of ZIF-90 and ZIF-90-NH2 2 2.4 Preparation of membranes 3 2.5 TAEA thermal modification of membranes 3 2.6 Characterization 3 2.7 Gas permeation tests 4 3 Results and discussion 4 3.1 ZIF-90 and ZIF-90-NH2 characterization 4 3.2 ZIF-90 and ZIF-90-NH2 based MMMs 5 3.2.1 Characterizations of membranes 5 3.2.2 Gas transport properties of membranes 7 3.3 TAEA thermal modification MMMs 8 3.3.1 Characterizations of membranes 8 3.3.2 Gas transport properties of membranes 9 3.4 Comparison of the performance with literature findings 10 4 Conclusions 11 CRediT authorship contribution statement 11 Declaration of competing interest 11 Data availability 11 Acknowledgements 11 Appendix A Supplementary data 11 References 11

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nonfiction