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Magnetic solid phase extraction of aminoglycosides residue in chicken egg samples using Fe3O4-GO-Agarose-Chitosan composite 1 1 Introduction 1 2 Experimental 2 2.1 Materials 2 2.2 HPLC-UV/vis analysis 2 2.3 Synthesis of composite adsorbent for aminoglycosides extraction 2 2.3.1 Synthesis of graphene oxide 2 2.3.2 Synthesis of iron oxide nanoparticles 2 2.3.3 Synthesis of magnetic graphene oxide 2 2.3.4 Preparation of Fe3O4-GO-agarose-chitosan composite film 2 2.4 Characterization of the synthesized composite 3 2.5 Real sample analysis 3 2.6 Regeneration studies 3 3 Results and discussion 3 3.1 X-ray diffraction analysis and vibrating sample magnetometry 3 3.2 FT-IR analysis 3 3.3 Scanning electron microscopy 3 3.4 Batch adsorption study 5 3.4.1 Kinetic study of MGO-Agr-Chi composite 6 3.5 Method validation 6 3.6 Real sample analysis and regeneration studies 7 3.7 Performance evaluation of the proposed method 7 4 Conclusion 7 Declaration of Competing Interest 8 Data availability 8 Acknowledgments 8 Appendix A Supplementary data 8 References 8
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- Language
- EN
- Category
- nonfiction
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