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Synthesis and characterization of Schiff base ligand-mutliwalled carbon nanotubes as mercury-free electrochemical sensor fo ... 1 1 Introduction 1 2 Experimental 2 2.1 Reagents 2 2.2 Synthesis of N,N′-bis(salicylaldehyde)-1,2-diaminobenzene (BSD) 2 2.3 Modification of BSD/MWCNTs 3 2.4 Electrochemical detection of Pb2+ and Hg2+ 3 2.5 Methods 3 3 Results and discussion 3 3.1 Fourier transform infrared spectroscopy (FT-IR) analysis 3 3.2 Proton nuclear magnetic resonance spectroscopy (1H NMR) analysis 3 3.3 Morphological of BSD/MWCNTs analysis on metal surfaces 3 3.4 Investigations of cyclic voltammogram and electrochemical impedance spectroscopy 5 3.5 Contemporaneously electrochemical activity for Pb2+ and Hg2+ on BSD/MWCNTs modified electrode 6 3.6 Determination of complex formation for Pb2+ and Hg2+ with BSD/MWCNTs 7 3.7 Assessment of Pb2+ and Hg2+using BSD/MWCNTs 8 3.8 Interferences for Pb2+ and Hg2+ ions on BSD/MWCNTs with various metal ions 8 3.9 Investigation of Pb2+ and Hg2+ in lake and ground water 9 4 Conclusion 9 Declaration of competing interest 9 Data availability 9 Acknowledgements 9 Appendix A Supplementary data 9 References 9
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It is typically read by self-directed learners exploring a subject in depth.
Common subject areas: history, science, philosophy, social sciences.
- Language
- EN
- Category
- nonfiction
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