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A molecularly imprinted electrochemical sensor with tunable electrosynthesized Cu-MOFs modification for ultrasensitive dete ... 1 1 Introduction 1 2 Experimental 2 2.1 Reagents and materials 2 2.2 Apparatus 2 2.3 Reductive electrosynthesis of Cu-MOFs 2 2.4 Preparation of MIP-base d electrochemical sensors 2 2.5 Optimization of IgG sensor 3 2.6 Assay performance evaluation of IgG sensor 4 2.7 Electrochemical examinations 4 3 Results and discussion 5 3.1 SEM characterization of MIP/CS/Cu-MOF/GCE 5 3.2 XRD characterization of MIP/CS/Cu-MOF/GCE 5 3.3 Electrochemical behavior of the prepared MIP/CS/Cu-MOF/GCE 5 3.4 Tunable electrochemistry of Cu-MOFs 7 3.4.1 SEM characterization of Cu-MOFs at different reduction potentials 7 3.4.2 Electrochemical behavior of Cu-MOFs at different reduction potentials 8 3.5 Analytical performance of MIP/CS/Cu-MOF/GCE 8 3.6 Selectivity, reproducibility and stability of MIP/CS/Cu-MOF/GCE 8 3.7 MIP/CS/Cu-MOF/GCE sensor efficiency of IgG determination in clinic blood samples 9 4 Conclusions 10 Declaration of Competing Interest 10 Acknowledgement 10 References 10

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nonfiction