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A thermodynamic approach to understand the partitioning of tetracycline family antibiotics in individual and mixed micellar systems 1 1 Introduction 1 2 Materials and methods 2 2.1 Materials 2 2.2 Isothermal titration calorimetry 3 2.3 Fluorescence spectroscopy 3 3 Results & Discussion 3 3.1 Drug partitioning in micellar HTAB 3 3.1.1 Interaction of doxycycline with HTAB micelles 3 3.1.2 Interaction of minocycline with HTAB micelles 5 3.1.3 Interaction of tetracycline with HTAB micelles 6 3.1.4 Interaction of oxytetracycline with HTAB micelles 6 3.2 Interaction of drugs in monomeric HTAB 6 3.3 Drug partitioning in micellar TX-100 7 3.3.1 Interaction of doxycycline with TX-100 micelles 7 3.3.2 Interaction of minocycline with TX-100 micelles 7 3.3.3 Interaction of tetracycline with TX-100 micelles 7 3.3.4 Interaction of oxytetracycline with TX-100 micelles 8 3.4 Interaction of drugs in monomeric TX-100 10 3.5 Drug partitioning in mixed micelles 10 3.6 Interaction of drugs in mixed monomers 11 3.7 Effects of tetracycline drugs on the micellization of HTAB, TX-100 and mixed surfactant 13 3.7.1 Micelles 13 3.8 Drug partitioning studies by pyrene fluorescence 13 3.9 Structure-property-ene

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nonfiction