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Synthesis, aggregation behavior and drug-binding interactions of fatty acid-imidazolium-based surface-active ionic liquids 1 1 Introduction 1 2 Materials and methods 2 2.1 Materials 2 2.2 Synthesis of ester-functionalized ethyl-substituted imidazolium SAILs 2 2.3 Characterization data 2 2.4 Determination of cmc of SAILs 3 2.4.1 Conductivity measurements 3 2.4.2 Probe-less UV–visible spectroscopy 3 2.4.3 Fluorescence measurements 3 2.5 Determination of aggregation number 3 2.6 Study of binding interactions of SAILs with anesthetic drug 3 2.6.1 Fluorescence spectroscopy 3 2.6.2 Differential UV–visible spectroscopy 3 2.7 Determination of size and shapes of the aggregates 3 2.7.1 Dynamic light scattering (DLS) 3 2.7.2 Transmission electron microscopy (TEM) 3 3 Results and discussion 4 3.1 Determination of critical micellar concentration (cmc) 4 3.2 Thermodynamics parameters of ester-functionalized SAILs 5 3.3 Effect of SAILs on the aggregation number of drug 8 3.4 Binding interactions study of SAILs with anesthetic drug 8 3.4.1 Fluorescence spectroscopy 8 3.4.2 Evaluation of partition parameters using differential spectroscopy 9 3.5 Determination of size and shapes of the aggregates 10

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EN

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nonfiction