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Foreword 0 Introduction 0 1 Scope 0 2 Normative references 0 3 Terms and definitions 0 4 Principle 0 5 Apparatus 0 6 Reagents 0 7 Preparation 0 7.1 General 0 7.2 Preparation of solutions 0 7.2.1 Sulphuric acid, 0,01 M — Impinger solution (trapping system 1) 0 7.2.2 Sulphuric acid, 0,1 M — Solution C (Ion Chromatography Eluent) 0 7.2.3 MSA 0,003 M — Solution A (Ion chromatography eluent) 0 7.2.4 Sulphuric acid, 0,01 M — Ammonium standards preparation 0 7.2.5 Hydrochloric acid, 0,05 M — Solution for GFP impregnation (trapping system 2) 0 7.2.6 Hydrochloric acid, 0,01 M — Extraction solution (trapping system 2) 0 7.3 Preparation of standards 0 7.3.1 Primary ammonium stock solution 0 7.3.2 Calibration standards 0 8 Sampling 0 9 Tobacco product preparation 0 10 Sample generation — Smoking of cigarettes 0 10.1 General 0 10.2 Smoking machine setup 0 10.2.1 General 0 10.2.2 Trapping system 1 — GFP and impinger traps 0 10.2.3 Trapping system 2 — Impregnated GFP 0 10.3 Smoking 0 11 Sample analysis 0 11.1 Preparation of sample 0 11.1.1 Extraction of GFP – Trapping system 1 0 11.1.2 Extraction of GFP – Trapping system 2 0 11.2 Determination 0 11.2.1 Ion chromatography operating conditions 0 11

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ISO

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