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1 Scope 7 2 Normative references 7 3 Terms and definitions 8 4 Symbols 8 5 General considerations 9 5.1 Limit of detection: table of risks 9 5.2 Limit of quantification: effect on repeatability r 9 5.3 Typically accepted values for limits of detection and quantification 10 6 Methods for determining limits of detection and quantification 11 6.1 Principles and summary of methods 11 6.2 Main method 1 – Determination of LD and LQ from matrix data from blank samples 12 6.2.1 Principle 12 6.2.2 Advantages of main method 1 13 6.2.3 Disadvantages of main method 1 13 6.2.4 Examples of applications of main method 1 13 6.3 Main method 2 – Determination of LD and LQ from the linearity of calibration data 14 6.3.1 Principle 14 6.3.2 Advantages of main method 2 15 6.3.3 Disadvantages of main method 2 15 6.3.4 Examples of applications 15 6.4 Main method 3 — Checking a given or prescribed quantification limit 15 6.4.1 Principle 15 6.4.2 Advantages of main method 3 16 6.4.3 Disadvantages of main method 3 16 6.4.4 Applications 16 6.5 Other methods 17 6.5.1 Horwitz method 17 6.5.2 Determination of the limit of detection from a qualitative analysis 17 7 Presentation of results 17 7.1 Minimum requirem

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RUTISHAUSER Sonia

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reference