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Cutting-edge advances on the stability and state diagram of pure β-lactose 1 1 Introduction 1 2 Materials and methods 2 2.1 Materials 2 2.2 Preparation of β-lactose (Lβ) 2 2.3 Determination of water sorption isotherms 3 2.4 Physicochemical characterization analysis 3 2.4.1 Raman spectroscopy 3 2.4.2 Identification of crystalline phases by X-ray diffraction 3 2.4.3 Scanning electron microscopy (SEM) 3 2.4.4 Thermal analysis by modulated differential scanning calorimetry (MDCS) 3 3 Results and discussion 4 3.1 Sorption isotherms 4 3.2 Chemical analysis 5 3.3 Microstructural identification 5 3.4 Morphological analysis 6 3.5 Thermal analysis by modulated differential scanning calorimetry 7 3.6 Equilibrium state diagram of Lβ 7 4 Conclusions 7 CRediT authorship contribution statement 8 Declaration of competing interest 8 Data availability 8 Acknowledgments 8 References 8

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Language

EN

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nonfiction