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Foreword 0 Introduction 0 1 Scope 0 2 Normative references 0 3 Terms and definitions 0 4 Principle 0 5 Interferences 0 6 Reagents and standards 0 6.1 Solvents for extraction and preparation of stock solutions 0 6.2 Reference SCCP stock solutions 0 6.3 Internal standard stock solutions from individual congeners 0 6.4 Calibration solutions 0 6.5 Extraction auxiliary and clean-up materials 0 7 Apparatus 0 8 Sampling and sample pretreatment 0 9 Procedure 0 9.1 Extraction with liquid-liquid extraction 0 9.2 Extraction with higher content of suspended matter 0 9.3 Extract clean-up 0 9.4 Measurement and integration of the chromatogram 0 9.5 Calibration 0 9.5.1 General 0 9.5.2 Basic calibration 0 9.5.3 Identification and quantification with mass fragment combinations 0 9.5.4 Calculation of the results 0 9.5.5 Quality checks for internal standardization 0 10 Expression of results 0 11 Test report 0 Annex A (normative) Independent quality control check solutions 0 Annex B (informative) Explanation of the calibration of the sum of SCCPs with multiple linear regression 0 Annex C (informative) Typical GC-MS conditions 0 Annex D (informative) Typical chromatograms of standard solutions and q
Who reads Water quality -- Determination of short-chain polychlorinated alkanes (SCCP) in water -- Method using gas chromatography-mass spectrometry (GC-MS) and negative-ion chemical ionization (NCI)?
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- Author
- ISO
- Language
- EN
- Category
- reference
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