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Foreword 0 1 Scope 0 2 Normative references 0 3 Terms and definitions 0 4 Principle 0 5 Interferences 0 5.1 Biases 0 5.2 Limitations 0 6 Reagents and standards 0 6.1 General 0 6.2 Preparation of solutions 0 7 Apparatus 0 8 Sampling 0 9 Procedure 0 9.1 Preparation of samples 0 9.1.1 General 0 9.1.2 Preparation of method blank sample 0 9.1.3 Preparation of laboratory control spike sample 0 9.1.4 Preparation of calibration control sample 0 9.1.5 Preparation of calibration standard solutions 0 9.1.6 Preparation of drinking water and freshwater sample 0 9.1.7 Sample preparation procedure with freeze/thaw cycles 0 9.2 Instrumental analysis by LC-MS/MS procedure 0 9.2.1 Instrument set-up parameters 0 9.3 Run processing and quality assurance 0 9.3.1 Run sequence 0 9.3.2 Run control operations / limits 0 10 Calibration 0 11 Evaluation and calculation of results 0 11.1 Identification and calculations 0 11.2 Calibration curve equation determination 0 11.3 Internal standard calculation 0 11.4 Internal standard recovery calculation 0 12 Expressing of results 0 13 Test report 0 Annex A (informative) Use of high resolution mass spectrometry detectors (HRMS) 0 Annex B (informative) Use of online

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ИСО

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reference