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New copper(II) μ-alkoxo-μ-carboxylato double-bridged complexes as models for the active site of catechol oxidase: synthesis ... 1 1. Introduction 1 2. Experimental 2 2.1. Synthesis of the schiff base ligand (H3L) 2 2.2. [{Cu2(L)}2][(μ–O2C–CO2] 1 2 2.3. [{Cu2(L)}2 (μ–O2C–(CH2)CO2] 2 2 2.4. [{Cu2(L)}2 (μ–O2C–(CH2)2–CO2] 3 3 2.5. [{Cu2(L)}2 (μ–O2C–C6H4–CO2] 4 3 2.6. Physical measurements 3 2.7. Catecholase activity 3 2.8. Superoxide dismutase (SOD) 3 2.9. Computational calculations 3 3. Results and discussion 4 3.1. Powder X-ray diffraction 4 3.2. Quantum chemistry 4 3.3. NMR spectra 5 3.4. FTIR spectral studies 6 3.5. UV-visible analysis 6 3.6. Electrochemistry of complexes 6 3.7. Epr studies of copper(II) tetranuclear complexes 8 3.8. Kinetics for 3, 5-di-tert-butyl catechol activity 8 3.9. SOD activity 10 3.10. Structure-activity relationship analysis 10 4. Conclusions 11 Declarations 11 Author contribution statement 11 Funding statement 11 Data availability statement 11 Declaration of interests statement 11 Additional information 11 Acknowledgements 11 References 11

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nonfiction