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All reactions were carried out under an argon atmosphere. Reagents were purchased at a high commercial quality (typically 97 % or higher) and used without further purification, unless otherwise stated. 1 H NMR and 13 C NMR spectra were recorded on Bruker spectrometers (at 400 or 500 MHz or at 100 or 125 MHz) and are reported relative to deuterated solvent signals (CDCl3: 1 H NMR = 7.24, 13 C NMR = 77.0, MeOD: 1 H NMR = 3.30, 13 C NMR = 49.0, DMSO-d6: 1 H NMR = 2.50, 13 C NMR = 39.5). The following abbreviations were used to explain the multiplicities: s = singlet, d = doublet, t = triplet, q = quartet, quint = quintet, dd = double doublet, dt = double triplet, dq = double quartet, m = multiplet, br = broad. Electrospray ionization mass spectrometry (ESI-MS) data were collected on triple-stage quadrupole instrument in a positive mode. Flash column chromatography was performed using reversed phase (100 Å, 20-40-micron particle size, RediSep® Rf Gold® Reversed-phase C18 or C18Aq) and silica on a CombiFlash® Rf 200i (Teledyne Isco, Inc.). LC/MS was performed using a Shimadzu LCMS-2020 Single Quadrupole utilizing a Kinetex 2.6 μm C18 100 Å (2.1 x 50 mm) column obtained from Phenomenex,

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Publisher

American Chemical Society (ACS)

Language

EN

Category

nonfiction