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## Table of Contents ■ Supplementary Methods ■ ■ Supplementary Methods ■ 1. Instrumentation and Chemicals NMR spectra were recorded on a Bruker AVANCE NEO 400N spectrometer, operating at 400 MHz for 1 H NMR, 100.6 MHz for 13 C NMR and Bruker Ultra Shield-300 (300 MHz), operating at ng at 300 MHz for 1 H NMR, 75 MHz for 13 C NMR. Chemical shift values for 1 H and 13 C are referenced to Me4Si and the residual solvent resonances, respectively. Chemical shifts were reported in d ppm. Mass spectra were obtained with JMS-T100TD (DART and ESI-TOF). TLC analyses were performed on commercial glass plates bearing 0.25-mm layer of Merck Silica gel 60F254. Silica gel (Wakosil ® 60, 64~210 μm) was used for column chromatography. Biotage Selekt was used for purification. IR spectra were measured with a Thermo Scientific iD7 ATR Accessory for the Thermo Scientific Nicolet iS5 FT-IR Spectrometer. Melting points were measured on a Stanford Research Systems MPA100. CV measurements were recorded with a Hokuto Denko HZ-7000 potentiostat. UV-Vis absorption spectra were recorded on a Shimadzu UV-1900. Fluorescence spectra were recorded on a Shimadzu RF-6000. Kessil A160W Tuna Blue (highest blue and inte

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Publisher

American Chemical Society (ACS)

Language

EN

Category

nonfiction