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One-pot synthesis of heteroaromatic acetals via selectfluor-mediated tandem reaction of methyl quinoline-2-carboxylate and ... 1 1. Introduction 1 2. Result and discussion 2 3. Conclusion 4 4. Experimental section 4 4.1. Material and instrumentation 4 4.2. General experimental procedures 4 4.2.1. General procedure for the preparation of methyl quinolin-2-formate 1 4 4.2.2. General procedure for the selectfluor-mediated tandem reaction 4 4.3. Physical and spectral data 4 4.3.1. Methyl quinoline-2-carboxylate (1a) 4 4.3.2. Methyl 5-fluoroquinoline-2-carboxylate (1b) 4 4.3.3. Methyl 6-fluoroquinoline-2-carboxylate (1c) 4 4.3.4. Methyl 6-chloroquinoline-2-carboxylate (1d) 5 4.3.5. Methyl 6-bromoquinoline-2-carboxylate (1e) 5 4.3.6. Methyl 5-iodoquinoline-2-carboxylate (1f) 5 4.3.7. Methyl 6-(trifluoromethyl)quinoline-2-carboxylate (1g) 5 4.3.8. Methyl 6-methylquinoline-2-carboxylate (1h) 5 4.3.9. Methyl 7-chloroquinoline-2-carboxylate (1i) 5 4.3.10. Methyl 8-fluoroquinoline-2-carboxylate (1j) 5 4.3.11. Methyl 8-chloroquinoline-2-carboxylate (1k) 5 4.3.12. Methyl 8-bromoquinoline-2-carboxylate (1l) 5 4.3.13. Methyl 8-methylquinoline-2-carboxylate (1m) 5 4.3.14. Methyl 5,6-difluoroquino

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nonfiction