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Di- and tetra-nuclear oxorhenium(V) complexes of benzoylthiourea derivative ligands: Synthesis, structural characterization ... 1 1 Introduction 1 2 Experimental 2 2.1 Instrumentation 2 2.2 Reagents 2 2.3 Synthesis and characterization 2 2.3.1 General procedure for the synthesis of ligands (H2L1,2) 2 2.3.2 General procedure for the synthesis of dinuclear oxorhenium(V) complexes 2 2.3.3 General procedure for the synthesis of tetranuclear oxorhenium(V) complexes 3 2.4 Catalytic activity test 3 3 Results and discussion 4 3.1 Synthesis 4 3.2 Crystal structure analysis 4 3.2.1 ReV2O2L22(OCH3)2] (Complex 2) 5 3.2.2 [ReV2O2L12-(μ-O)2-ReV2O2L12] (Complex 1′) 7 3.3 Catalytic activity 8 4 Conclusions 11 Funding 11 Disclosure statement 11 CRediT authorship contribution statement 11 Declaration of Competing Interest 11 Acknowledgements 11 Appendix A Supplementary data 11 References 11
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- Language
- EN
- Category
- nonfiction
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