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HF-Pyridine in Azobenzene-Cytidine Synthesis by Yong-Sheng Wei is a document available to read on EtoBox.

What is HF-Pyridine in Azobenzene-Cytidine Synthesis about?

The document describes a synthetic procedure for azobenzene-modified cytidine, starting with a coupling reaction of silyl-protected chloride-substituted cytidine and azobenzene-aniline in DMF, yielding an orange solid with an 83% yield after purification. The product was characterized using 1H NMR, 13C NMR, and HRMS, confirming the molecular structure. A subsequent step involved treating the azobenzene-modified cytidine with hydrogen fluoride-pyridine complex under controlled conditions.

Author

Yong-Sheng Wei

Language

EN