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Synthesis of super-hydrophobic CuO/ZnO layered composite nano-photocatalyst 1 1 Introduction 1 2 Experimental 2 2.1 The preparation of CuO nanowires 2 2.2 Growth of ZnO nanostructures 2 2.3 Synthesis of CuO/ZnO composite nanostructures 2 2.4 Super-hydrophobic treatment 2 2.5 Characterization 2 2.6 Photocatalytic test 3 3 Results and discussion 3 3.1 The preparation of CuO nanowires 3 3.2 The preparation of CuO/ZnO nanostructures 3 3.2.1 Effect of zinc sources on ZnO growth 3 3.2.2 Effect of reaction time on ZnO growth 5 3.2.3 Effect of reaction solution concentration on ZnO growth 6 3.2.4 Effect of HMT ratio on ZnO growth 6 3.3 Formation mechanism of CuO/ZnO nanostructures 7 3.4 Super-hydrophobicity of CuO/ZnO nanostructures 10 3.5 Photocatalysis and stable super-hydrophobicity 10 4 Conclusion 10 CRediT authorship contribution statement 11 Declaration of competing interest 11 References 11

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EN

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nonfiction