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Surface-active agents and detergents -- Determination of water content -- Karl Fischer methods by GARCIA Miguel is a reference work available to read on EtoBox.

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1 Scope 5 2 Normative references 5 3 Terms and definitions 5 4 Principle 5 5 Test methods 6 5.1 General 6 5.2 Volumetric titration method 6 5.2.1 Principle 6 5.2.2 Reagents 6 5.2.3 Apparatus 6 5.2.4 Sampling 7 5.2.5 Procedure 7 5.2.5.1 General 7 5.2.5.2 Determination of the water equivalent of Karl Fischer reagent (5.2.2.2) 7 5.2.5.3 Determination of water content 8 5.2.5.3.1 General 8 5.2.5.3.2 General method 8 5.2.5.3.2.1 Determination 8 5.2.5.3.2.2 Expression of results 9 5.2.5.3.3 Dissolution method 9 5.2.5.3.3.1 Determination 9 5.2.5.3.3.2 Expression of results 9 5.3 Coulometric titration method 10 5.3.1 Principle 10 5.3.2 Reagents 10 5.3.3 Apparatus 10 5.3.4 Sampling 12 5.3.5 Procedure 12 5.3.5.1 Calibration of titration device 12 5.3.5.2 Determination of water content 12 5.3.5.3 Expression of results 13 6 Precision 13 6.1 Precision of the volumetric titration method 13 6.1.1 Repeatability 13 6.1.2 Reproducibility 13 6.2 Precision of the coulometric titration method 13 6.2.1 Repeatability 13 6.2.2 Reproducibility 14 7 Test report 14

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Author

GARCIA Miguel

Language

EN

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reference