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This document describes the Zimmermann-Reinhard method for determining the concentration of iron in a sample through a volumetric titration with potassium permanganate. The method involves (1) reducing all Fe(III) to Fe(II) with stannous chloride, (2) removing the excess stannous chloride with mercuric chloride, and (3) adding a Zimmermann-Reinhard reagent before the titration with permanganate to enhance the detection of the endpoint and compensate.

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