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Contents page 1. General information S2 2. Experimental details and characterization data of new compounds S2 3. References S22 4. Copies of NMR Spectra S23 S2 1. General Information. All reactions were carried out with anhydrous solvents in oven-dried glassware with magnetic stirring under argon unless otherwise stated. The chemical reagents were used as supplied except where noted. Analytical thin layer chromatography (TLC) was performed on precoated plates of silica gel (0.25-0.3 mm, Shanghai, China). The TLC plates were visualized by exposure to ultraviolet light or staining with a sulfuric acid-ethanol solution. Silica gel column chromatography was conducted on silica gel AR (100-200 mesh, Shanghai, China). Optical rotations (OR) were recorded with a Rudolph Research Analytical Autopol I automatic polarimeter. NMR spectra were recorded with a Bruker Avance III 400, Bruker Avance III 500, or Bruker Avance III 600 spectrometer. The 1 H and 13 C NMR spectra were calibrated against the residual proton and carbon signals of the solvents as internal references (CDCl 3 : δ H = 7.26 ppm and δ C = 77.2 ppm; CD 3 OD: δ H = 3.31 ppm and δ C = 49.0 ppm). Multiplicities are quoted as singl

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Publisher

American Chemical Society (ACS)

Language

EN

Category

nonfiction