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Multifunctional halloysite and hectorite catalysts for effective transformation of biomass to biodiesel 1 1 Introduction 1 2 Experimental 3 2.1 Materials 3 2.2 Syntheses 3 2.2.1 Synthesis of Hal-NH2 and Ht-NH2 nanomaterials 3 2.2.2 Synthesis of Hal-TBAI@ZnO and Ht-TBAI@ZnO catalysts 3 2.3 Catalytic tests 3 2.4 Procedure for catalyst recycling 3 3 Results and discussion 3 3.1 Synthesis and characterization of Hal-TBAI@ZnO nanomaterials 3 3.2 Catalytic tests with Hal-TBAI@ZnO 4 3.2.1 Optimization of reaction conditions: application of DOE Method 5 3.2.2 Recycling experiments 6 3.2.3 Literature comparison 6 3.2.4 Catalytic tests on waste lipids 7 3.3 Esterification of FFAs in the presence of different clay minerals 7 3.3.1 Modification of Ht 8 3.3.2 Catalytic activity of Ht-TBAI@ZnO nanomaterial 8 4 Conclusions 8 Funding 9 CRediT authorship contribution statement 9 Declaration of Competing Interest 9 Data availability 9 Acknowledgment 9 Appendix A Supplementary data 9 References 9

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Language

EN

Category

nonfiction