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Unless otherwise stated, all reactions were magnetically stirred and conducted in oven-dried (90 °C) or flame-dried glassware in anhydrous solvents under Ar, applying standard Schlenk techniques. Solvents and liquid reagents, as well as solutions of solid or liquid reagents were added via syringes, stainless steel or polyethylene cannulas through rubber septa or through a weak Ar counter-flow. Solid reagents were added through a weak Ar counter-flow. Cooling baths were prepared in Dewar vessels, filled with ice/water (0 °C), cooled acetone (> 78 °C) or dry ice/acetone (78 °C). Heated oil baths were used for reactions requiring elevated temperatures. Solvents were removed under reduced pressure at 40 °C using a rotary evaporator, and unless otherwise stated, the remaining compound was dried in high vacuum (10 3 mbar) at ambient temperature. All given yields are isolated yields of chromatographically and NMR spectroscopically pure materials (95%), unless otherwise stated. ## Chemicals Chemicals were purchased from commercial suppliers (including abcr, Acros, Alfa Aesar, Fluorochem, Merck, and TCI) and used without further purification unless otherwise stated. Et3N was distilled fr

Who reads Azine Activation via Silylium Catalysis?

Publisher

American Chemical Society (ACS)

Language

EN

Category

nonfiction