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This document provides a procedure for synthesizing potassium tris(oxalato)aluminate(III) trihydrate. The synthesis involves adding aluminum powder to an aqueous solution of potassium hydroxide, then adding oxalic acid dihydrate to form a gelatinous precipitate of aluminum hydroxide. Upon continued addition of oxalic acid and warming, the solution becomes clear indicating formation of the tris(oxalato)aluminate(III) ion. Crystals are obtained by cooling and adding ethanol. An average 70% yield of white crys

Author

Felipe Vilches

Language

EN