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Ammonium Di(carboxylato)triphenylstannates. Crystal Structures Of Dicyclohexylammonium Bis(trifluoroacetato) Triphenylstannate, Diisopropylammonium Bis[bis(n,n-dimethylthio-carbamoylthio)acetato]-triphenylstannate And 2,2'-iminodipyridinium Bis(trifluoroacetato)triphenylstannate by Seik Weng Ng; James M. Hook is a Chemistry article available to read on EtoBox.

What is Ammonium Di(carboxylato)triphenylstannates. Crystal Structures Of Dicyclohexylammonium Bis(trifluoroacetato) Triphenylstannate, Diisopropylammonium Bis[bis(n,n-dimethylthio-carbamoylthio)acetato]-triphenylstannate And 2,2'-iminodipyridinium Bis(trifluoroacetato)triphenylstannate about?

The crystal structures of dicyclohexylammonium bis(trifluoroacetato)triphenylstannate (1), diisopropylammonium bis[(A',i'V-dimethylthiocarbamoylthio)acetato]tnphenylstannate (2) and 2,2'iminodipyridinium bis(chlorodifluoroacetato)triphenylstannate (3) consist of ammonium cations and stannate anions that are linked by Ν Ο hydrogen bonds into linear chains [(1) 2.784(4) A; (2) 2.780(5) A, 2.950(6) A; (3) 2.779(7) A, 3.073(8) A], The tin atom in the five-coordinate stannates shows /rara-C 3 Sn0 2 trigonal bipyramidal coordination [(1) Zc-sn-c 360.0(4)°, O-Sn-O 174.1(1)°, Sn-0 2.258(2) A; (2) Zc-sn-c 359.9(6)°, O-Sn-O 178.8(1)°, Sn-0 2.213(3) A , 2.227(3) A; (3) I C -s"-c 359.5(6)°, O-Sn-O 179.7(2)°; Sn-0 2.194(5), 2.310(5) A], The 5, s " chemical shifts in the solid-state " 9 Sn MAS NMR spectra of (1), ( 2) and tetramethylammonium bis(trifluoroacetato)triphenylstannate are of the order of -300 ppm relative to tetramethyltin; the spectra yield axially-symmetric chemical shift tensors and -1 asymmetry parameters.

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Author

Seik Weng Ng; James M. Hook

Published

1999

Field

Chemistry (Physical Sciences)