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Microwave-assisted Synthesis of Acrylamide Grafted Polymeric Blend of by Narendra Kumar Pandey; Asha Gandhi; Surajpal Verma; Sachin Kumar Singh; Bimlesh Kumar; Bala Vikash; CK Sudhakar is a Materials Science article available to read on EtoBox.

What is Microwave-assisted Synthesis of Acrylamide Grafted Polymeric Blend of about?

## Objective: In this study, fenugreek gum (isolated from fenugreek seed) was modified into a grafted form using a microwave-assisted method. Acrylamide was used as a monomer, and ceric ammonium nitrate (CAN), potassium persulfate (KPS), and ammonium persulfate (APS) were used as redox initiators. ## Methods: The experimental design (Taguchi OA) was used to optimize the synthesis of the grafted copolymer of fenugreek gum. In this model, seven independent variables were selected on the basis of their preliminary study. These were monomer concentration (X1), gum concentration (X2), initiator concentration (X3), irradiation power (X4), speed (X5), time (X6), temperature (X7), and three response variables as % yield (Y1), % grafting (Y2), and % grafting efficiency (Y3) were identified. The optimized copolymers of grafted gum were characterized by Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), differential scanning calorimetry (DSC), NMR studies, surface morphology and swelling index. ## Results: The yield of fenugreek gum after extraction was found to be 55.99±0.015% w/w. The percentage grafting of 50.20±4.0, along with grafting efficiency of 83.7±0.1, was obt

Who reads Microwave-assisted Synthesis of Acrylamide Grafted Polymeric Blend of?

Author

Narendra Kumar Pandey; Asha Gandhi; Surajpal Verma; Sachin Kumar Singh; Bimlesh Kumar; Bala Vikash; CK Sudhakar

Publisher

Bentham Science Publishers Ltd.

Published

2022

Language

EN

Field

Materials Science (Physical Sciences)