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The first general synthesis of 3‐iodo‐4‐ R ‐furazans by Aleksei B. Sheremetev; Julia L. Shamshina; Dmitry E. Dmitriev; Denis V. Lyubetskii; Mikhail Yu. Antipin is a Chemistry article available to read on EtoBox.
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## Abstract The first general synthetic route has been developed for the convenient preparation of iodofurazans. The approach was accomplished by one‐pot diazotization‐iodation reaction of appropriate aminofurazans. A combination of sodium nitrite and iodine in organic solvent under anhydrous conditions as the reaction conditions allowed to solve problem in iodofurazans preparation. The investigation of the substituent's influence on NMR data of the iodofurazans has been carried out. The X‐ray crystal structure of the 3‐amino‐4‐iodofurazan **1d** is reported. © 2004 Wiley Periodicals, Inc. Heteroatom Chem 15:199–207, 2004; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/hc.20007
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- Author
- Aleksei B. Sheremetev; Julia L. Shamshina; Dmitry E. Dmitriev; Denis V. Lyubetskii; Mikhail Yu. Antipin
- Publisher
- John Wiley and Sons; Hindawi Limited; John Wiley & Sons Inc.; Wiley (ISSN 1042-7163)
- Published
- 2004
- Language
- EN
- Field
- Chemistry (Physical Sciences)