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Insights of precursor phase transition of (Cu-Zn-Al)/γ-Al2O3 hybrid catalyst for one step dimethyl ether synthesis from syngas 1 1 Introduction 1 2 Materials and methods 2 2.1 Chemicals and materials 2 2.2 Catalyst preparation 2 2.2.1 Preparation of methanol synthesis catalyst 2 2.2.2 Preparation of Cu-Zn hybrid catalyst 3 2.3 Catalyst characterization 3 2.4 Catalytic activity 3 3 Results and discussion 4 3.1 Catalyst characterization 4 3.1.1 X-ray diffraction analysis (XRD) 4 3.1.2 N2 physisorption study 5 3.1.3 Cu surface area and particle size measurement of Cu-Zn hybrid catalysts 5 3.1.4 Reducibility profile of Cu-Zn hybrid catalysts 5 3.1.5 Surface acidity of Cu-Zn hybrid catalysts 6 3.1.6 Morphology aspects of Cu-Zn hybrid catalysts 7 3.2 Catalytic activity 8 3.2.1 Effect of temperature 8 3.2.2 Effect of space velocity and syngas ratio 9 3.2.3 Catalyst stability 10 4 Conclusion 11 CRediT authorship contribution statement 11 Declaration of Competing Interest 11 Acknowledgments 11 Appendix A Supporting information 11 References 11

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Language

UND

Category

nonfiction