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Simultaneous determination of five tetracycline and macrolide antibiotics in feeds using HPCE by Jing Tong; Qinxiong Rao; Kui Zhu; Zhigang Jiang; Shuangyang Ding is a Chemistry article available to read on EtoBox.

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## Abstract This work demonstrates the potential of HPCE in the analysis of antibiotics in a complex matrix such as feedstuffs. Using 20 mM citric acid–40 mM Na~2~HPO~4~ buffer (pH 2.65), the five antibiotics, tetracycline, oxytetracycline, doxycycline, tilmicosin, and tylosin were successfully separated at 30 kV in a 64.5 cm×75 μm id capillary. Good repeatability, stability, and reliability of the method were supported by 70%, and the limit of detection of the five analytes was 0.5–1 mg/kg. It was for the first time that a capillary electrophoretic method was employed to simultaneously detect five tetracycline and macrolide antibiotics in animal feeds.

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Author

Jing Tong; Qinxiong Rao; Kui Zhu; Zhigang Jiang; Shuangyang Ding

Publisher

John Wiley and Sons; Wiley (John Wiley & Sons); John Wiley & Sons Ltd.; Wiley (ISSN 1615-9306)

Published

2009

Language

EN

Field

Chemistry (Physical Sciences)