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Foreword 0 1 Scope 0 2 Normative references 0 3 Terms and definitions 0 4 Principle 0 5 Reagents and materials 0 6 Apparatus 0 7 Sampling 0 8 Sample preparation 0 9 Procedure for determination of PAHs from fats and oils: General method 0 9.1 Preliminary remarks 0 9.2 Blank 0 9.3 Determination of recovery values (without matrix) 0 9.4 Extraction (liquid/liquid extraction) 0 9.5 Purification on C18-bonded phase cartridge (solid/liquid extraction) 0 9.6 Purification on Florisil-bonded phase cartridge (solid/liquid extraction) 0 10 Procedure for determination of PAHs from fats and oils: Method specific for coconut oil 0 10.1 First extraction (liquid/liquid extraction) 0 10.2 Second extraction (liquid/liquid extraction) 0 10.3 Purification on C18-bonded phase cartridge (solid/liquid extraction) 0 10.4 Purification on Florisil-bonded phase cartridge (solid/liquid extraction) 0 11 High-performance liquid chromatography (HPLC) 0 11.1 Operating conditions 0 11.2 Detection parameters 0 11.3 Analysis of samples and standards 0 11.4 Confirmation of the presence of PAHs 0 12 Expression of results 0 13 Precision 0 13.1 Interlaboratory test 0 13.2 Repeatability 0 13.3 Reproducibility 0 14 Test re

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ISO

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EN

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reference