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Synthesis and structure activity relationship of the first class of LXR inverse agonists 1 1 Introduction 1 2 Results and discussion 2 2.1 Chemistry 2 2.2 Structure activity relationship (SAR) studies 3 2.3 Molecular dynamics simulations 4 2.4 Biological activity 6 3 Conclusions 6 4 Experimental 7 4.1 Chemistry 7 4.1.1 N-(4-Bromobenzyl)-2,4,6-trimethylbenzenesulfonamide (10) 7 4.1.2 2,4,6-Trimethyl-N-((3′-(methylsulfonyl)-[1,1′-biphenyl]-4-yl)methyl)benzenesulfonamide (11) 8 4.1.3 General method A: Preparation of compounds 4, 6, 7, 12–27. 8 4.1.3.1 2,4,6-Trimethyl-N-((3′-(methylsulfonyl)-[1,1′-biphenyl]-4-yl)methyl)-N-((5-(trifluoro-methyl)-furan-2-yl)methyl)ben ... 8 4.1.3.2 Ethyl 5-((2,4,6-trimethyl-N-((3′-(methylsulfonyl)-[1,1′-biphenyl]-4-yl)methyl)phenyl- sulfonamido)methyl)furan-2-ca ... 8 4.1.3.3 N-(3-Bromophenethyl)-2,4,6-trimethyl-N-((3′-(methylsulfonyl)-[1,1′-biphenyl]-4-yl)methyl)-benzenesulfonamide (7) 9 4.1.3.4 5-((2,4,6-Trimethyl-N-((3′-(methylsulfonyl)-[1,1′-biphenyl]-4-yl)methyl)phenyl-sulfonamido)methyl)furan-2-carboxyli ... 9 4.1.3.5 N-(4-(Tert-butyl)benzyl)-2,4,6-trimethyl-N-((3′-(methylsulfonyl)-[1,1′-biphenyl]-4-yl)-methyl)benzenesulfonamide (13) 10 4.1.3.6 N-(
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