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Nickel nanoparticles were synthesized by reduction of nickel acetylacetonate in a monosurfactant system. They were used as catalyst for the growth of multiwalled carbon nanotubes by the catalytic decomposition of methane at 500 c. A detailed characterization of the magnetic properties of the Ni nanoparticle. And Ni nanotubes embedded is hereby presented. Both the systems show superparamagnetic behaviour above the blocking temperature TB.

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