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## I. General Information General Reagent Information: Cesium fluoride (TCI catalog #C2204) and 18-crown-6 (Chem-Impex catalog #03901) were purchased from Fisher Scientific and stored in a nitrogen-filled glovebox prior to use. Benzyltrimethylsilane (catalog #QA-9873) was purchased from Combi-Blocks. 2,2,6,6-Tetramethyl-1-piperidinyloxy (TEMPO) was purchased from Millipore Sigma (catalog #426369, purified by sublimation, 99%). Anhydrous solvents: dimethyl sulfoxide (catalog #276855), tetrahydrofuran (catalog #186562), 1,2-dimethoxyethane (catalog #259527) and N,Ndimethylformamide (catalog #227056) were used as received from Millipore Sigma. Tetrahydrofuran and dichloromethane solvents were deoxygenated and dried by passage over packed columns of neutral alumina and copper (II) oxide under positive pressure of nitrogen. All other commercially available reagents and solvents were purchased from Alfa Aesar, Combi-Blocks, Acros Organics or Millipore Sigma and used as received. Column chromatography was performed using 40-63 μm silica gel (SiliaFlash® F60 from Silicycle) or Basic Alumina 60-325 Mesh (Fisher Chemical Cat. # A941-500). Preparative thin-layer chromatography (PTLC) was perf

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Publisher

American Chemical Society (ACS)

Language

EN

Category

nonfiction