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The objective of the experiment was to synthesize tert-butyl chloride through a unimolecular nucleophilic substitution using tert-butanol and concentrated hydrochloric acid. It was observed that upon shaking the reaction mixture, the phases separated, and the addition of calcium chloride made this separation more noticeable. When neutralizing with sodium bicarbonate, bubbles of carbon dioxide were formed. Finally, tert-butyl chloride and water were obtained as products.
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