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Synthesis, thermal and spectral studies of first-row transition metal complexes with girard P reagent-based ligand by Usama El-Ayaan; I.M. Kenawy; Y.G. Abu El-Reash is a Chemistry article available to read on EtoBox.

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A new series of first-row transition metal complexes with 1-acetylpyridinium chloride-4-benzoyl thiosemicarbazide (H 2 GPBzIT) have been prepared and characterized by elemental analysis, spectroscopic and magnetic measurements. The proton-ligand ionization constants were determined potentiometrically using Irving-Rossotti technique. The stability constants of complexes were also calculated and were found in agreement with the seq uence of stability constants of Irving and Williams. Thermal stability and degradation kinetics have been measured using thermogravimetric analyzer. Kinetic parameters were obtained for each stage of thermal degradation of complexes using Coats-Redfern method.

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Author

Usama El-Ayaan; I.M. Kenawy; Y.G. Abu El-Reash

Publisher

Elsevier Science; Elsevier ; Elsevier Ltd.; Pergamon Press Ltd.; Elsevier BV (ISSN 1386-1425)

Published

2007

Language

EN

Field

Chemistry (Physical Sciences)