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Analysis of the 1H and 13C{1H} NMR Spectral Parameters of the Tear Gases α-Chloroacetophenone, Dibenz[b,f][1,4]oxazepine, and 2-Chlorobenzylidene Malononitrile by Markku Mesilaakso is a Chemistry article available to read on EtoBox.
What is Analysis of the 1H and 13C{1H} NMR Spectral Parameters of the Tear Gases α-Chloroacetophenone, Dibenz[b,f][1,4]oxazepine, and 2-Chlorobenzylidene Malononitrile about?
The 'H and '3C{'H) NMR spectra of the tear gases a-chloroacetophenone, dibenz[b,f] [ 1,4)oxazepine and 2chlorobenzylidene malononitrile were recorded in CDCl, , CD,CI, and (CD,),CO and analysed. Assignments of the resonances were confirmed by homonuclear and heteronuclear correlation spectroscopy. Detailed 'H spectral parameters were determined by iterative analysis. The conformations of dibenz [ S , f ] [ 1,4] oxazepine and 2chlorobenzylidene malononitrile were determined on the basis of the long-range coupling constants 4J(a,0rth0), 'J(a,meta) and 6J(a,para). Use of the 'H spectral parameters of dibenz[b,f][1,4]oxazepine for simulation of a reference spectrum is demonstrated for a test sample.
Who reads Analysis of the 1H and 13C{1H} NMR Spectral Parameters of the Tear Gases α-Chloroacetophenone, Dibenz[b,f][1,4]oxazepine, and 2-Chlorobenzylidene Malononitrile?
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- Author
- Markku Mesilaakso
- Publisher
- John Wiley and Sons; Wiley (John Wiley & Sons); John Wiley & Sons Inc.; John Wiley and Sons Ltd; Wiley (ISSN 0749-1581)
- Published
- 1996
- Language
- EN
- Field
- Chemistry (Physical Sciences)