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Electrochemical synthesis of Nickel(II) Complexes of schiff bases: The crystal structure of 2,2′-bipyridine bis{2-[(phenyl)iminomethyl]pyrrolato}nickel(II) by J. A. Castro; J. E. Vilasanchez; J. Romero; J. A. Garcia-Vazquez; M. L. Duran; Prof. Dr. A. Sousa; E. E. Castellano; J. Zukerman-Schpector is a Chemistry article available to read on EtoBox.

What is Electrochemical synthesis of Nickel(II) Complexes of schiff bases: The crystal structure of 2,2′-bipyridine bis{2-[(phenyl)iminomethyl]pyrrolato}nickel(II) about?

The electrochemical oxidation of anodic nickel in acetonitrile solution containing both a) a Schiff base HL derived from H-pyrrole-2-carbaldehyde and a substituted aniline, and b) a nitrogen ligand (1,lO-phenanthroline (phen), 2,2 '-bipyridine (bipy) or pyridine (py)) yielded the mixed complexes NiL,phen, NiL, bipy and NiL, \* (py),. The crystal structure of 2,2'-bipyridine bis~2-[(phenyl)iminomethyl]pyrrolato)nickel(II) was determined by X ray diffraction. Crystals are triclinic space group Pi, with four molecules in the unit cell of dimensions a = 12.316(1), b = 13.169(4), c = 17.251(3) A , a = 82.67(3)', /3 = 83.6611)" and y = 87.34(2)", and consist of monomeric molecules in which the central NiN, unit has a distorted octahedral geometry.

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Author

J. A. Castro; J. E. Vilasanchez; J. Romero; J. A. Garcia-Vazquez; M. L. Duran; Prof. Dr. A. Sousa; E. E. Castellano; J. Zukerman-Schpector

Publisher

John Wiley and Sons; Wiley (John Wiley & Sons); Wiley - V C H Verlag GmbbH & Co.; Wiley (ISSN 0372-7874)

Published

1992

Language

EN

Field

Chemistry (Physical Sciences)