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Preparation and condensation reactions of a new light-fluorous Mukaiyama reagent: reliable purification with fluorous solid phase extraction for esters and amides by Masato Matsugi; Masakazu Hasegawa; Daisuke Sadachika; Sachina Okamoto; Mami Tomioka; Yoshimi Ikeya; Araki Masuyama; Yuji Mori is a Chemistry article available to read on EtoBox.

A modified light-fluorous Mukaiyama reagent bearing a C 8 F 17 tag was prepared and examined in ester and amide forming condensation reactions. Following the reactions, the desired product was effectively separated from the fluorous pyridone by-product using a simple fluorous solid phase extraction.

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Author
Masato Matsugi; Masakazu Hasegawa; Daisuke Sadachika; Sachina Okamoto; Mami Tomioka; Yoshimi Ikeya; Araki Masuyama; Yuji Mori
Publisher
Elsevier Science; Elsevier ; Elsevier Ltd.; Elsevier BV (ISSN 0040-4039)
Published
2007
Language
EN
Field
Chemistry (Physical Sciences)