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MAS-NMR at very high temperatures by Leo van Wüllen; Georg Schwering; Ernst Naumann; Martin Jansen is a Chemistry article available to read on EtoBox.

What is MAS-NMR at very high temperatures about?

We report MAS-NMR experiments at temperatures of approx. 1200 K using a CO(2) laser as the heating device. An internal NMR thermometer based on the (7)Li T1 data of Li(0.24)La(0.54)TiO(3) is used for temperature calibration. Using this setup, temperatures as high as 1191 K could be reached under MAS conditions as confirmed by the melting of Li(2)B(4)O(7) at 1191 K which could be followed by (7)Li-MAS-NMR.

Who reads MAS-NMR at very high temperatures?

Author

Leo van Wüllen; Georg Schwering; Ernst Naumann; Martin Jansen

Publisher

Elsevier Science; Elsevier ; Elsevier Inc.; Elsevier BV (ISSN 0926-2040)

Published

2004

Language

EN

Field

Chemistry (Physical Sciences)