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Microwave-Assisted Synthesis of Pt Nanoparticles via Liquid-Phase Polyol Reaction for Catalytic Volatile Organic Compound Elimination by Yunzi Xin; Taku Nagata; Kunihiko Kato; Takashi Shirai is a Materials Science article available to read on EtoBox.
What is Microwave-Assisted Synthesis of Pt Nanoparticles via Liquid-Phase Polyol Reaction for Catalytic Volatile Organic Compound Elimination about?
The microwave-assisted synthesis of functional metal nanoparticles (NPs) has gained considerable interest because of the shorter reaction period, significantly reduced energy consumption, and lower environmental impact compared to conventional heating. Herein, we elucidate the microwave-assisted synthesis of Pt NPs via liquid-phase polyol reaction based on a detailed investigation of the reaction dynamics during synthesis and its correlation with NP growth and crystallinity formation. The reduction behavior of Pt precursor under temperature scale is initially clarified, whose results suggest that precursor reduction plays an important role in deciding the crystallinity of Pt NPs corestate, that is polycrystalline Pt NPs with twinned crystal planes in microwave-assisted fast heating, and single crystalline Pt NPs in microwave-assisted slow heating. In addition, through a systematic comparison with oil-bath-induced conventional heating under identically controlled experimental conditions, the effect of microwave irradiation on the synthesis of the Pt NPs is also clarified. We also study the volatile oxidation products generated in polyol processes and derived a reaction mechanism dis
Who reads Microwave-Assisted Synthesis of Pt Nanoparticles via Liquid-Phase Polyol Reaction for Catalytic Volatile Organic Compound Elimination?
It is typically read by researchers, students, and practitioners in Materials Science.
- Author
- Yunzi Xin; Taku Nagata; Kunihiko Kato; Takashi Shirai
- Publisher
- American Chemical Society (ACS)
- Published
- 2022
- Language
- EN
- Field
- Materials Science (Physical Sciences)