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On-line coupling of solid-phase extraction to gas chromatography with fast solvent vaporization and concentration in an open injector liner: Analysis of pesticides in aqueous samples by Ryoichi Sasano; Takayuki Hamada; Mitsuhiro Kurano; Masahiro Furuno is a Chemistry article available to read on EtoBox.

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The purpose of this study is to combine solid-phase extraction (SPE) with gas chromatography (GC) for the fully automated determination of pesticides and herbicides in aqueous samples. The interface technique employed for connecting SPE with GC was fast solvent vaporization and concentration in an open injector liner. The interface device consisted of the programmed-temperature vaporizing injector without using the packing material in the liner and the target compounds were concentrated around the inlet of the GC capillary column. This avoided the degradation of target compounds, and no precise control of the injecting speed was required, when an automatic SPE system was connected to GC-MS. The aqueous samples used in this system were prepared by spiking 29 kinds of pesticide and herbicide compounds, which are regulated by the Ministry of Health and Welfare of the Japanese National government, in purified water and river water, to a resulting concentration of 1 mg / l. Employing this system, the recoveries and RSDs (n56) of most compounds were greater than 75% and within 10%, respectively. From the results of this study, we found that on-line automatic SPE and capillary GC-MS equip

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Author

Ryoichi Sasano; Takayuki Hamada; Mitsuhiro Kurano; Masahiro Furuno

Publisher

Elsevier Science; Elsevier ; Elsevier BV (ISSN 1873-3778)

Published

2000

Language

EN

Field

Chemistry (Physical Sciences)