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Oxidative C–H Sulfonylation of Hydrazones Enabled by Electrochemistry by Qi-Liang Yang; Ping-Ping Lei; Hai-Ming Guo; Er-Jun Hao; Bei-Ning Zhang; Hong-Hao Zhou; Wan-Wan Li is a Chemistry article available to read on EtoBox.
What is Oxidative C–H Sulfonylation of Hydrazones Enabled by Electrochemistry about?
## Abstract An efficient electrochemical oxidative C(sp2)–H sulfonylation of aldehyde hydrazones is described. A variety of sodium sufinates or sulfinic acids participate effectively in this protocol, which provides facile access to an array of alkyl and aromatic sulfonylated hydrazones with up to 96% yield. Large-scale synthesis and product derivatization show the potential utility of this methodology. Preliminary mechanistic investigations including radical-inhibition, electricity on/off experiments, and cyclic voltammetry support a radical pathway.
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It is typically read by researchers, students, and practitioners in Chemistry.
- Author
- Qi-Liang Yang; Ping-Ping Lei; Hai-Ming Guo; Er-Jun Hao; Bei-Ning Zhang; Hong-Hao Zhou; Wan-Wan Li
- Publisher
- Georg Thieme Verlag KG
- Published
- 2023
- Field
- Chemistry (Physical Sciences)